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2021 Vol.53, Issue 5 Preview Page
Separation of Cellulose from Rice Hull

왕겨 바이오매스에서 셀룰로오스 분리

Audrey Zahra1
,
Seo-Kyoung Lim2
,
Soo-Jeong Shin23†
Audrey Zahra 1
,
임서경 2
,
신수정 23†
1Department of Wood & Paper Science, Chungbuk National University, Cheongju, Chungbuk 28644
2Nature Costech Inc. Cheongju 28444
3Department of Wood & Paper Science, Chungbuk National University, Cheongju, Chungbuk 28644
1충북대학교 목재종이과학과, 대학원생
2네이처코스텍(주), 연구원
3충북대학교 목재종이과학과, 교수
†Corresponding author: E-Mail: soojshin@cbnu.ac.kr (Address: Department of Wood & Paper Science, Chungbuk National University, Cheongju 28644, Republic of Korea)
30 October 2021. pp. 28-34
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Abstract

Rice hull was proposed as an alternative raw material for cellulose production. Rice hull has cellulose (38.6+/-0.1%), xylan (12.8+/-0.1%), lignin (22.7+/-0.7%), extractives (7.9+/-0.4%), and inorganic (13.2+/-0.8%).Inorganic was selectively removed using moderate alkaline extraction, and lignin was degraded via oxidation with chlorine dioxide or hypochlorite. In this study, dilute acid hydrolysis was used to selectively remove hemicellulose, resulting in purer cellulose and better yield. Xylan was selectively removed using sulfuric acid at various acid concentrations (0.25–1 N), reaction time (60–120 min), and temperature (100–120°C) with desilicated and delignified biomass. The reaction conditions for ＞90% cellulose purity were 120°C and 1.0 N sulfuric acids. Increasing the reaction duration resulted in higher cellulose purity, with the greatest purity being 96.1% at 1.00 N sulfuric acid, 120°C, and 120-min reaction time.

Keywords
Rice hull
cellulose
dilute acid hydrolysis
xylan
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Information
  • Publisher :Korea Technical Association of The Pulp and Paper Industry
  • Publisher(Ko) :한국펄프종이공학회
  • Journal Title :Journal of Korea TAPPI
  • Journal Title(Ko) :펄프종이기술
  • Volume : 53
  • No :5
  • Pages :28-34
  • Received Date : 2021-09-14
  • Revised Date : 2021-10-07
  • Accepted Date : 2021-10-08
  • DOI :https://doi.org/10.7584/JKTAPPI.2021.10.53.5.28
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